OPTIMIZED SYNTHESIS AND CHARACTERIZATION OF CARBOXYMETHYLCELLULOSE DERIVED FROM SUGARCANE BAGASSE LIGNOCELLULOSE (Saccharum officinarum L.): COMPREHENSIVE FTIR AND QUALITY STANDARD ANALYSES L. O. A. Rasydy, D. Pratiwi, P. P. M. Rahayu, T. M. Fakih, A. A. Setiawan, R. S. A. Wahid, L. Hamidu Rasayan Journal of Chemistry, 2025 Bagasse is a fibrous waste material derived from sugarcane (Saccharum officinarum L.) that can be useful in producing carboxymethyl cellulose (CMC). This study synthesized CMC from bagasse using NaOH concentrations of 25%, 35%, and 45%, along with 20% trichloroacetic acid (TCA), to produce high-quality CMC. The results revealed that the CMC synthesized with 35% NaOH exhibited properties closely aligning with the standards reported by the Food and Agriculture Organization (FAO). The drying loss, moisture content, pH, viscosity, NaCl content, purity, and degree of substitution were 3.1%, 5.247%, 6.91, 688.3 cP, 0.25%, 99.74%, and 1.08, respectively. Fourier-transform infrared analysis confirmed the functional groups characteristic of CMC, with prominent peaks at 3121.9 cm⁻¹ (OH group), 2886.5 cm⁻¹ (C-H group), 1663.6 cm⁻¹ (COO⁻ group), and 1029 cm⁻¹ (-O- group). These findings suggest that bagasse can be effectively utilized to produce high-quality CMC and potentially convert waste into value-added products.
Chemoprofiling of active n-hexane fraction as alpha-glucosidase inhibitors from kanunang (Cordia myxa L.) leaves from enrekang south sulawesi Journal of Global Pharma Technology, 2019
Qualitative and quantitative test of total flavonoid buni fruit (Antidesma bunius (L.) Spreng) with UV-Vis spectrophotometry method La Hamidu, Aktsar Roskiana Ahmad, Ahmad Najib Pharmacognosy Journal, 2018 The aim of this research is to determine of total flavonoid content in the Buni fruit (Antidesma bunius L. Spreng) extract. The extract was produced by stratified maceration method with the different solvent, i.e n-Hexane, Ethyl acetate and ethanol. The analysis of chemical compound using chemical reagent and Thin Layer Chromatography (TLC) method. The method is used to determines total flavonoid contains Buni fruit (Antidesma bunius L.) extract was based on the amount of Rutin Equivalent (RE) were used. The result shows that the flavonoid content higher in the n-Hexane extract is 10.72 %, then ethyl acetate extract is 7.9 % and 3.56 % ethanol extract was counted to or as a Rutin.
RECENT SCHOLAR PUBLICATIONS
Concentration-dependent antibacterial activity of Ruellia tuberosa L. leaf ethanol extract against Propionibacterium acnes ATCC 6919 I Yani, L Hamidu, ML Meiliana Pharmacy Reports 5 (3), 112-112 , 2025 2025
In Silico Screening of Chemical Compound Activity as an α-Glucosidase Inhibitor from Sweet Flag Rhizome (Acorus calamus L.) A Najib, M Fawwaz, A Ismail, L Hamidu Jurnal Fitofarmaka Indonesia 12 (3) , 2025 2025 Citations: 2
Potensi Antioksidan Daun Lobi-Lobi (Flacourtia inermis Roxb): Penentuan Kadar Total Flavonoid dan Fenolik L Hamidu, V Septiani, ML Meiliana, A Najib Jurnal Fitofarmaka Indonesia 12 (1), 31-36 , 2025 2025 Citations: 1
OPTIMIZED SYNTHESIS AND CHARACTERIZATION OF CARBOXYMETHYLCELLULOSE DERIVED FROM SUGARCANE BAGASSE LIGNOCELLULOSE (Saccharum officinarum L.): COMPREHENSIVE FTIR AND QUALITY … LOA Rasydy, D Pratiwi, PPM Rahayu, TM Fakih, AA Setiawan, ... RASĀYAN Journal of Chemistry 18 (4), 2087-2093 , 2025 2025
Uji Oligosakarida Ekstrak Tepung Buah Semu Jambu Mete (Anacardium occidentale L.) Terhadap Pertumbuhan Baketri Lactobacillus casei Sebagai Altenatif Prebiotik R Elsa, N Nuraini, L Hamidu Jurnal Fitofarmaka Indonesia 11 (2), 73-78 , 2024 2024 Citations: 2
AKTIVITAS ANTIPIRETIK EKSTRAK RIMPANG BENGLE (Zingiber purpureum Roxb) PADA TIKUS PUTIH JANTAN YANG DIINDUKSI DENGAN VAKSIN DTP-HB-Hib MA Kusniawati, I Kurniawati, L Hamidu Jurnal Farmagazine 11 (2), 42-49 , 2024 2024 Citations: 2
Daun Cempaka Kuning (Michelia Champaca Linn) Sebagai Kandidat Penghambat Enzim Α-Glukosidase Secara In Silico R Amalia, ML Meiliana, L Hamidu Jurnal Fitofarmaka Indonesia 11 (1), 23-32 , 2024 2024 Citations: 2
Postprandial Bioassay and Radical Scavenging on n-Hexane Fraction of Cordia myxa L. Leaf V Handayani, AR Ahmad, NRK Nisaa, L Hamidu, A Najib Jurnal Fitofarmaka Indonesia 9 (3), 13-18 , 2022 2022 Citations: 2
Determination of total phenolic content of the stem bark extract of nyirih (Xylocarpus granatum J. Koeing) using UV-VIS spectrophotometry method A Aswar, A Malik, L Hamidu, A Najib Jurnal Fitofarmaka Indonesia 8 (3), 12-17 , 2021 2021 Citations: 14
Potensi ekstrak buah buni (Antidesma bunius (L) Spreng) sebagai inhibitor enzim α-glukosidase L Hamidu, P Simanjuntak, RT Dewi Jurnal Fitofarmaka Indonesia 7 (1), 27-30 , 2020 2020 Citations: 9
MAHONI (Switenia mahagoni (L.) Jacq) Herbal Untuk Penyakit Diabetes LH Aktsar Roskiana Ahmad, Virsa Handayani, Reski Amriati Syarif, Ahmad Najib 2019
Qualitative and quantitative test of total flavonoid buni fruit (Antidesma bunius (L.) Spreng) with UV-Vis spectrophotometry method L Hamidu, AR Ahmad, A Najib Pharmacognosy Journal 10 (1), 60-63 , 2018 2018 Citations: 44
MOST CITED SCHOLAR PUBLICATIONS
Qualitative and quantitative test of total flavonoid buni fruit (Antidesma bunius (L.) Spreng) with UV-Vis spectrophotometry method L Hamidu, AR Ahmad, A Najib Pharmacognosy Journal 10 (1), 60-63 , 2018 2018 Citations: 44
Determination of total phenolic content of the stem bark extract of nyirih (Xylocarpus granatum J. Koeing) using UV-VIS spectrophotometry method A Aswar, A Malik, L Hamidu, A Najib Jurnal Fitofarmaka Indonesia 8 (3), 12-17 , 2021 2021 Citations: 14
Potensi ekstrak buah buni (Antidesma bunius (L) Spreng) sebagai inhibitor enzim α-glukosidase L Hamidu, P Simanjuntak, RT Dewi Jurnal Fitofarmaka Indonesia 7 (1), 27-30 , 2020 2020 Citations: 9
In Silico Screening of Chemical Compound Activity as an α-Glucosidase Inhibitor from Sweet Flag Rhizome (Acorus calamus L.) A Najib, M Fawwaz, A Ismail, L Hamidu Jurnal Fitofarmaka Indonesia 12 (3) , 2025 2025 Citations: 2
Uji Oligosakarida Ekstrak Tepung Buah Semu Jambu Mete (Anacardium occidentale L.) Terhadap Pertumbuhan Baketri Lactobacillus casei Sebagai Altenatif Prebiotik R Elsa, N Nuraini, L Hamidu Jurnal Fitofarmaka Indonesia 11 (2), 73-78 , 2024 2024 Citations: 2
AKTIVITAS ANTIPIRETIK EKSTRAK RIMPANG BENGLE (Zingiber purpureum Roxb) PADA TIKUS PUTIH JANTAN YANG DIINDUKSI DENGAN VAKSIN DTP-HB-Hib MA Kusniawati, I Kurniawati, L Hamidu Jurnal Farmagazine 11 (2), 42-49 , 2024 2024 Citations: 2
Daun Cempaka Kuning (Michelia Champaca Linn) Sebagai Kandidat Penghambat Enzim Α-Glukosidase Secara In Silico R Amalia, ML Meiliana, L Hamidu Jurnal Fitofarmaka Indonesia 11 (1), 23-32 , 2024 2024 Citations: 2
Postprandial Bioassay and Radical Scavenging on n-Hexane Fraction of Cordia myxa L. Leaf V Handayani, AR Ahmad, NRK Nisaa, L Hamidu, A Najib Jurnal Fitofarmaka Indonesia 9 (3), 13-18 , 2022 2022 Citations: 2
Potensi Antioksidan Daun Lobi-Lobi (Flacourtia inermis Roxb): Penentuan Kadar Total Flavonoid dan Fenolik L Hamidu, V Septiani, ML Meiliana, A Najib Jurnal Fitofarmaka Indonesia 12 (1), 31-36 , 2025 2025 Citations: 1
Concentration-dependent antibacterial activity of Ruellia tuberosa L. leaf ethanol extract against Propionibacterium acnes ATCC 6919 I Yani, L Hamidu, ML Meiliana Pharmacy Reports 5 (3), 112-112 , 2025 2025
OPTIMIZED SYNTHESIS AND CHARACTERIZATION OF CARBOXYMETHYLCELLULOSE DERIVED FROM SUGARCANE BAGASSE LIGNOCELLULOSE (Saccharum officinarum L.): COMPREHENSIVE FTIR AND QUALITY … LOA Rasydy, D Pratiwi, PPM Rahayu, TM Fakih, AA Setiawan, ... RASĀYAN Journal of Chemistry 18 (4), 2087-2093 , 2025 2025
MAHONI (Switenia mahagoni (L.) Jacq) Herbal Untuk Penyakit Diabetes LH Aktsar Roskiana Ahmad, Virsa Handayani, Reski Amriati Syarif, Ahmad Najib 2019
