Postdoctoral Research Fellow at the OTIC - Offshore Technology Innovation Centre, an applied research center at the University of São Paulo, Brazil.
Research interests:
- Recycling of Li-ion batteries
- Electric vehicles
- Extraction of critical metals
- Hydrometallurgy
- Circular Economy and Sustentability
- Life Cycle Assessment (LCA)
- Circularity Index
- FPSO units
- Project Management
RESEARCH, TEACHING, or OTHER INTERESTS
Chemical Engineering, Materials Science, Renewable Energy, Sustainability and the Environment, Multidisciplinary
Characterization of Lithium-Ion Batteries from Recycling Perspective towards Circular Economy Lucas Fonseca Guimarães, Jorge Alberto Soares Tenório, Mentore Vaccari, Denise Crocce Romano Espinosa, Amilton Barbosa Botelho Junior Minerals, 2024 Recycling processes of lithium-ion batteries used in electric and hybrid vehicles are widely studied today. To perform such recycling routes, it is necessary to know the composition of these batteries and their components. In this work, three pouch and three cylindrical LIBs were discharged, dismantled, and characterized, having their compositions known and quantified. The dismantling was performed using scissors, pliers, and a precision cutter equipment. The organic liquid electrolyte was quantified via mass loss after it evaporated at 60 °C for 24 h. The separators were analyzed using Fourier-transform infrared spectroscopy (FTIR), and the cathode and anode active materials were analyzed using a scanning electronic microscope coupled to an energy-dispersive spectroscope (SEM-EDS), X-ray diffraction (XDR), and energy-dispersive X-ray fluorescence spectrometry (EDXRF). All LIBs were identified by type (NCA, NMC 442, NMC 811, LCO, and two LFP batteries), and a preliminary economic evaluation was conducted to understand their potential economic value (in USD/t). Both results (characterization and preliminary economic evaluation) were considered to discuss the perspective of recycling towards a circular economy for end-of-life LIBs.
Electric car battery: An overview on global demand, recycling and future approaches towards sustainability Lívia Salles Martins, Lucas Fonseca Guimarães, Amilton Barbosa Botelho Junior, Jorge Alberto Soares Tenório, Denise Crocce Romano Espinosa Journal of Environmental Management, 2021 Li-ion batteries are daily present in our electronic devices. These batteries are used in electric and hybrid vehicles supporting the current agreements to decrease greenhouse gas emissions. As a result, the electric vehicle demand has increased in the world. As Li-ion batteries are composed of critical metals in which there is a risk of interruption of supply in the medium term, recycling is the key to a sustainable future without internal combustion vehicles. Understanding the current scenario and future perspectives is important for strategies of new battery design, recycling routes and reverse logistics, as well as policies for sustainable development. This paper presents an overview of current and future vehicles used worldwide. An increase from 1.3 to 2 billion vehicles is expected worldwide until 2030; an outstanding demand will occur mainly in BRICS countries. The data demonstrated a correlation between the number of vehicles in use and GDP. Patents and processes designed for recycling Li-ion batteries and the new developments on pyro-, hydro-, and bio-metallurgical routes have been revised. The manuscript describes the importance and benefits of recycling as regards the supply of critical metals and future trends towards a circular economy.
RECENT SCHOLAR PUBLICATIONS
Sustainable Recovery of Valuable Metals from NMC 811 Batteries: A Hydrometallurgical Approach with Life Cycle Assessment LF Guimarães, M Vaccari, ABB Junior, DCR Espinosa TMS Annual Meeting & Exhibition, 161-171 , 2026 2026
Recycling of Li-ion batteries: hydrometallurgical flowchart, multivariate analysis, and life cycle assessment LF Guimaraes, CM Rebello, IBR Nogueira, M Vaccari, DCR Espinosa, ... Elsevier , 2026 2026 Citations: 1
Advancing Hydrometallurgical Recycling of Spent Lithium-Ion Batteries: An AI-Based Readliness and Sustainability Assessment DS Premathilake, LF Guimarães, DCR Espinosa, JAS Tenório, M Vaccari, ... 2025 Citations: 9
Characterization of Lithium-Ion Batteries from Recycling Perspective towards Circular Economy LF Guimarães, JAS Tenório, M Vaccari, DCR Espinosa, ... Minerals 14 (9), 878 , 2024 2024 Citations: 7
Reciclagem de baterias de Li-ion tipo NMC 811 para obtenção de metais críticos LF Guimarães Universidade de São Paulo (USP) , 2024 2024
The Characterization of Li-ion Batteries and the Importance of the Recycling Processes: Guimarães, Botelho Junior, and Espinosa LF Guimaraes, AB Botelho Junior, DCR Espinosa Jom 75 (9), 3622-3631 , 2023 2023 Citations: 13
Sulfuric acid leaching of metals from waste Li-ion batteries without using reducing agent LF Guimarães, ABB Junior, DCR Espinosa Minerals Engineering 183, 107597 , 2022 2022 Citations: 135
Electric car battery: An overview on global demand, recycling and future approaches towards sustainability LS Martins, LF Guimarães, ABB Junior, JAS Tenório, DCR Espinosa Journal of environmental management 295, 113091 , 2021 2021 Citations: 443
MOST CITED SCHOLAR PUBLICATIONS
Electric car battery: An overview on global demand, recycling and future approaches towards sustainability LS Martins, LF Guimarães, ABB Junior, JAS Tenório, DCR Espinosa Journal of environmental management 295, 113091 , 2021 2021 Citations: 443
Sulfuric acid leaching of metals from waste Li-ion batteries without using reducing agent LF Guimarães, ABB Junior, DCR Espinosa Minerals Engineering 183, 107597 , 2022 2022 Citations: 135
The Characterization of Li-ion Batteries and the Importance of the Recycling Processes: Guimarães, Botelho Junior, and Espinosa LF Guimaraes, AB Botelho Junior, DCR Espinosa Jom 75 (9), 3622-3631 , 2023 2023 Citations: 13
Advancing Hydrometallurgical Recycling of Spent Lithium-Ion Batteries: An AI-Based Readliness and Sustainability Assessment DS Premathilake, LF Guimarães, DCR Espinosa, JAS Tenório, M Vaccari, ... 2025 Citations: 9
Characterization of Lithium-Ion Batteries from Recycling Perspective towards Circular Economy LF Guimarães, JAS Tenório, M Vaccari, DCR Espinosa, ... Minerals 14 (9), 878 , 2024 2024 Citations: 7
Recycling of Li-ion batteries: hydrometallurgical flowchart, multivariate analysis, and life cycle assessment LF Guimaraes, CM Rebello, IBR Nogueira, M Vaccari, DCR Espinosa, ... Elsevier , 2026 2026 Citations: 1
Sustainable Recovery of Valuable Metals from NMC 811 Batteries: A Hydrometallurgical Approach with Life Cycle Assessment LF Guimarães, M Vaccari, ABB Junior, DCR Espinosa TMS Annual Meeting & Exhibition, 161-171 , 2026 2026
Reciclagem de baterias de Li-ion tipo NMC 811 para obtenção de metais críticos LF Guimarães Universidade de São Paulo (USP) , 2024 2024